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. 2018 Sep 3;74(Pt 9):877–894. doi: 10.1107/S2059798318009191

Table 6. Magnitudes of metrology changes.

Changes after each cycle of indexing and refinement using the expanding method are shown. Cycle 1: result after refining initial indexing solutions. Cycles 2–4: results after reindexing using the metrology of the previous cycle and re-refining using the expanding method. Shift: mean ± standard deviation of the magnitude of shifts in the xy plane (orthogonal to the beam vector). As an example, during cycle 1 the four quadrants moved 138 ± 111 µm on average. z Offsets: shifts along the z axis (equivalent to the detector distance). As the detector is constrained to be coplanar, all groups move the same amount. τ1: mean ± standard deviation of the rotation around the z axis. All values are relative to the parent frame.

  Level Shift (µm) z Offsets (µm) τ1 (°)
Cycle 1 Detector 56.3 ± 0.0 99.3 0.0 ± 0.0
Quadrants 138.3 ± 110.7 −118.1 0.2 ± 0.2
Sensors 53.7 ± 53.5 37.2 0.2 ± 0.1
Cycle 2 Detector 0.4 ± 0.0 −42.8 0.0 ± 0.0
Quadrants 3.8 ± 1.5 −18.0 0.0 ± 0.0
Sensors 9.8 ± 6.3 71.0 0.0 ± 0.0
Cycle 3 Detector 0.1 ± 0.0 −84.0 0.0 ± 0.0
Quadrants 1.6 ± 0.5 3.6 0.0 ± 0.0
Sensors 11.1 ± 6.1 86.0 0.0 ± 0.0
Cycle 4 Detector 0.2 ± 0.0 −92.2 0.0 ± 0.0
Quadrants 1.5 ± 0.7 3.3 0.0 ± 0.0
Sensors 9.0 ± 6.3 90.9 0.0 ± 0.0