Table 2.

¹H (600 MHz) and ¹³C (155 MHz) NMR Data of 3 in CDCl₃

no.	δc	δH (mult, J (Hz))	no.	δc	δH (mult, J (Hz))
1	108.1		1″	79.8
2	154.6		2″	132.9	5.54 d (10.2)
3	97.3		3″	129.4	5.44 br d (10.2)
4	161.3		4″	37.5	1.95 m
5	104.1		5″a	23.3	1.85 m
6	160.2		5″b		1.66 br dd (12.8, 6.2)
7	25.8	2.90 dd (11.5, 5.4)	6″	35.9	1.91 m
8	191.7	9.95 s	7″	29.6	1.63 s
9	26.4	5.34 t (8.2)	8″	31.9	1.67 m
10a	40.9	2.07 m	9″	19.4	0.90 d (6.8)
10b		1.79 m	10″	18.3	0.89 d (6.8)
11	26.4	1.47 m	1‴	104.8
12	22.6	0.87 d (6.6)	2‴	166.1
13	22.9	0.93 d (6.6)	3‴	110.7
1′	75.2		4‴	162.7
2′	131.2	5.80 d (10.2)	5‴	91.8	5.88 s
3′	134.6	5.97 dd (10.2, 4.5)	6‴	160.9
4′	40.6	1.98 m	7‴	210.0
5′a	20.3	1.61 m	8‴	46.0	3.64 sext (6.6)
5′b		1.38 ddd (20.9, 14.8, 6.6)	9‴	16.7	1.16 d (6.7)
6′	32.0	1.85 m	10‴a	27.3	1.82 m
7′	25.6	1.32 s	10‴b		1.40 m
8′	31.6	1.66 m	11‴	12.0	0.86 t (7.2)
9′	21.3	0.98 d (6.8)	2‴–OH		14.73 s
10′	21.0	1.00 d (6.8)	4‴-OH		8.97 s
6-OH		13.82 s	6‴-OMe	55.3	3.80 s