Table 1.
PAHs | R2 | LOD (μg/kg) | LOQ (μg/kg) | Recovery (%)a | Inter-day | Intra-day | ||
---|---|---|---|---|---|---|---|---|
Accuracy (%)b | CV (%)c | Accuracy (%)b | CV (%)c | |||||
1-NN | 0.9993 | 0.116 | 0.353 | 104.61 ± 1.89 | 109.66 | 2.24 | 98.62 | 1.71 |
2NN | 0.9994 | 0.128 | 0.387 | 109.64 ± 1.84 | 106.61 | 6.87 | 102.19 | 2.85 |
2-NF | 0.9978 | 0.099 | 0.300 | 96.95 ± 2.49 | 93.44 | 6.32 | 92.74 | 6.85 |
9-NA | 0.9987 | 0.166 | 0.502 | 107.10 ± 1.87 | 98.98 | 1.10 | 99.49 | 1.19 |
3-NF | 0.9979 | 0.119 | 0.361 | 109.49 ± 1.99 | 108.95 | 3.04 | 107.07 | 1.99 |
1-NP | 0.9970 | 0.115 | 0.349 | 98.88 ± 3.7 | 107.12 | 8.83 | 96.72 | 4.92 |
6-NC | 0.9986 | 0.136 | 0.411 | 94.58 ± 4.79 | 99.66 | 5.04 | 99.27 | 8.92 |
aRecovery was evaluated in samples spiked with 10 μg/kg
bAccuracy (%) = [1 − (mean concentration measured-concentration spiked)/concentration spiked] × 100
cCV (coefficient of variation, %) = (SD/mean) × 100