Table 3.
Identification of phyto-constituents in ethanolic extract of C. citratus leaves using GC–MS.
Ret. time | Area % | IUPAC name of compound | Mol formular | Mol. wt. |
---|---|---|---|---|
6.92 | 0.2126 | Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.alpha.)- | C9H18 | 126.2392 |
9.14 | 0.2154 | 2-Acetylcyclopentanone | C7H10O2 | 126.1531 |
9.30 | 0.4783 | 1,6-Octadien-3-ol, 3,7-dimethyl- | C10H18O | 154.2493 |
OR Linalool | ||||
10.47 | 2.6532 | 4H-Pyran-4-one, 2,3-dihydro-3,5-dihydroxy-6-methyl- | C6H8O4 | 144.1253 |
10.65 | 0.5139 | Cyclooctane, ethenyl- | C10H18 | 138.2499 |
10.88 | 0.2167 | Furan-2-carbohydrazide, N2-(1-methylhexylideno)- | ||
11.02 | 0.7758 | 7-Oxabicyclo[4.1.0]heptane, 1-methyl-4-(1-methylethenyl)- | C10H16O | 152.2334 |
11.87 | 0.2083 | Oxiranecarboxaldehyde, 3-methyl-3-(4-methyl-3-pentenyl)- | C10H16O2 | 168.2328 |
11.93 | 0.2702 | Benzofuran, 2,3-dihydro- | C8H8O | 120.1485 |
12.29 | 6.6959 | 2,6-Octadienal, 3,7-dimethyl-, (Z)- | C10H16O | 152.2334 |
12.49 | 0.6401 | Geraniol | C10H18O | 154.2493 |
12.60 | 2.545 | |||
12.96 | 9.4115 | Citral | C10H16O | 152.2334 |
13.10 | 1.1612 | Epoxy-linalooloxide | ||
13.20 | 1.1323 | |||
13.44 | 0.3872 | Cyclopentane, (1-methylethyl)- | C8H16 | 112.2126 |
13.69 | 0.4762 | 2-Methoxy-4-vinylphenol | C9H10O2 | 150.1745 |
13.88 | 0.5025 | Bicyclo[2.2.2]octan-1-amine | ||
13.98 | 0.3829 | 3-Cyclopropylcarbonyloxydodecane | ||
14.49 | 0.217 | Triallylsilane | C9H16Si | 152.3088 |
14.58 | 0.1855 | 3-Heptanol, 2-methyl- | C8H18O | 130.2279 |
14.64 | 0.1943 | 1,5-Heptadiene, 3,3-dimethyl-, (E)- | ||
14.95 | 0.8738 | Geranyl acetate | C12H20O2 | 196.2860 |
15.17 | 0.2231 | Cyclopropanemethanol,.alpha.,2-dimethyl-2-(4-methyl-3-pentenyl)-, [1.alpha.(R*),2.alpha.]- | ||
15.30 | 0.514 | Vanillin | C8H8O3 | 152.1473 |
15.65 | 0.3534 | 3,5-Heptadienal, 2-ethylidene-6-methyl- | C10H14O | 150.2176 |
16.09 | 0.4413 | Adamantane | C10H16 | 136.2340 |
16.40 | 0.4469 | 3-Cyclopentylpropionic acid, but-3-yn-2-yl ester | ||
16.59 | 0.4452 | 2-Propanol, 1,1,1-trichloro-2-methyl- | C4H7Cl3O | 177.457 |
16.95 | 0.9541 | 2,6-Octadienal, 3,7-dimethyl-, (Z)- | C10H16O | 152.2334 |
17.44 | 0.7992 | 3-Cyclohexene-1-acetaldehyde,.alpha.,4-dimethyl- | C10H16O | 152.2334 |
17.76 | 0.6387 | 3-n-Propyl-2-pyrazolin-5-one | C6H10N2O | 126.1564 |
17.85 | 0.3297 | 4-Methyl-5H-furan-2-one | C5H6O2 | 98.0999 |
18.11 | 0.3635 | Dodecanoic acid | C12H24O2 | 200.3178 |
19.00 | 0.1681 | 1-Methyl-3-n-propyl-2-pyrazolin-5-one | C7H12N2O | 140.1830 |
19.21 | 0.4101 | Selina-6-en-4-ol | ||
19.76 | 0.1779 | 2-(2-Hydroxyethylthio)propionic acid | ||
20.89 | 0.2064 | Phenylacetylformic acid, 4-hydroxy-3-methoxy- | ||
21.25 | 0.3042 | Tetradecanoic acid | C14H28O2 | 228.3709 |
21.45 | 0.2678 | Benzene, 1,1׳-ethylidenebis- | C14H14 | 182.2610 |
21.56 | 0.2124 | Pyridine, 4-[(1,1-dimethylethyl)thio]- | ||
22.30 | 0.3018 | p-Hydroxycinnamic acid, ethyl ester | ||
23.02 | 0.3948 | 2-Propenoic acid, 3-(4-hydroxy-3-methoxyphenyl)- | C10H10O4 | 194.1840 |
23.63 | 0.5611 | p-Fluoroethylbenzene | C8H9F | 124.1555 |
24.32 | 5.9637 | n-Hexadecanoic acid | C16H32O2 | 256.4241 |
24.64 | 1.1441 | Hexadecanoic acid, ethyl ester | C18H36O2 | 284.4772 |
25.05 | 0.3111 | Heptadecanoic acid | C17H34O2 | 270.4507 |
25.47 | 0.3151 | 3-Methyl-2-butenoic acid, 2-tridecyl ester | ||
26.23 | 0.7845 | Phytol | C20H40O | 296.5310 |
26.30 | 1.6582 | Diboroxane, triethyl[(4-methyl-2-pyridyl)amino]- | ||
26.62 | 3.8736 | 9,12-Octadecadienoic acid (Z,Z)- | C18H32O2 | 280.4455 |
26.71 | 3.6845 | 9,12,15-Octadecatrienoic acid, (Z,Z,Z)- | C18H30O2 | 278.4296 |
26.79 | 0.1683 | Cyclooctene, 3-ethenyl- | ||
26.87 | 0.9543 | Linoleic acid ethyl ester | C20H36O2 | 308.4986 |
26.97 | 0.988 | Ethyl 9,12,15-octadecatrienoate | ||
27.11 | 0.2389 | p-Menth-2-en-9-ol, trans- | ||
27.25 | 0.3594 | Octadecanoic acid, ethyl ester | C20H40O2 | 312.5304 |
27.44 | 0.2377 | 5,9-Undecadien-2-one, 6,10-dimethyl-, (E)- | C13H22O | 194.3132 |
27.57 | 0.2752 | Naphtho[2,1-b:3,4-b׳]difuran, 2,3,8,9-tetrahydro-2,9-dimethyl- | ||
27.77 | 0.4932 | Cyclohexanol, 5-methyl-2-(1-methylethenyl)- | C10H18O | 154.2493 |
28.62 | 0.2172 | 1,6,10,14-Hexadecatetraen-3-ol, 3,7,11,15-tetramethyl-, (E,E)- | C20H34O | 290.4834 |
29.28 | 0.4722 | Eicosanoic acid | C20H40O2 | 312.5304 |
29.65 | 0.2219 | Methyl 19-methyl-eicosanoate | ||
30.77 | 0.3075 | 9-Tricosene, (Z)- | C23H46 | 322.6113 |
31.86 | 0.527 | |||
34.22 | 0.2424 | |||
30.82 | 0.2058 | Heptadecane | C17H36 | 240.4677 |
30.95 | 0.237 | Hexadecanoic acid, 2-hydroxy-1-(hydroxymethyl)ethyl ester | C19H38O4 | 330.5026 |
31.39 | 0.5588 | Dichloroacetic acid, heptadecyl ester | ||
31.91 | 0.6148 | Hexacosane | C26H54 | 366.7070 |
32.79 | 0.2052 | Cyclohexane, 1,1׳-[4-(3-cyclohexylpropyl)-1,7-heptanediyl]bis- | C28H52 | 388.7125 |
32.92 | 1.2801 | 1-Nonadecene | C19H38 | 266.5050 |
32.98 | 1.9114 | Tetracosane | C24H50 | 338.6538 |
34.00 | 3.8594 | |||
36.85 | 3.8693 | |||
37.81 | 2.8508 | |||
38.92 | 2.0079 | |||
33.21 | 0.8589 | Butane, 2,2-bis(5-acetyl-2-thienyl)- | ||
34.32 | 0.1678 | Squalene | C30H50 | 410.7180 |
34.98 | 4.4543 | Nonacosane | C29H60 | 408.7867 |
35.21 | 0.2288 | Nonadecyl heptafluorobutyrate | ||
35.26 | 0.2462 | Heptacosyl acetate | ||
35.93 | 4.1869 | Triacontane | C30H62 | 422.8133 |
36.15 | 0.2301 | Triacontyl acetate | C32H64O2 | 480.8494 |
37.29 | 0.4097 | dl-.alpha.-Tocopherol | C29H50O2 | 430.7061 |
38.01 | 0.2942 | Benzene, 1-nitro-4-(phenylthio)- | C12H9NO2S | 231.270 |
38.37 | 0.3256 | Campesterol | C28H48O | 400.6801 |
38.74 | 0.5393 | Stigmasterol | C29H48O | 412.6908 |
38.81 | 0.3692 | 1,2,3,4-4H-Isoquinolin-1,3-dione, 4,4,5,6,8-pentamethyl- | ||
39.46 | 1.3421 | .gamma.-Sitosterol | C29H50O | 414.7067 |
39.97 | 0.8629 | 2-Furancarboxamide, N-[3-methyl-1-(phenylmethyl)-1H-pyrazol-5-yl]- | ||
40.21 | 1.9876 | Tetratriacontane | C34H70 | 478.9196 |
40.48 | 0.2395 | 9,19-Cyclolanost-24-en-3-ol, (3.beta.)- | C30H50O | 426.7174 |
41.09 | 0.4235 | 4-[5-(3,4-Diethoxy-benzyl)-[1,2,4]oxadiazol-3-yl]-furazan-3-ylamine | ||
41.48 | 0.6734 | Cannabidiol | C21H30O2 | 314.4617 |
41.73 | 0.8292 | Eicosane | C20H42 | 282.5475 |
43.54 | 0.3269 | |||
41.94 | 0.5473 | Cyclopropane-1-carboxamide, 2-butyl-N-(5,6,7,8-tetrahydro-7,7-dimethyl-5-oxoquinazolin-2-yl)- | ||
42.67 | 0.382 | 3-Methoxy-17beta-(O-nitrobenzoyloxy)-estra-1,3,5(10)-triene | ||
43.30 | 0.1722 | 2-(Acetoxymethyl)-3-(methoxycarbonyl)biphenylene |