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. 2018 May 20;43(2):108–113. doi: 10.1584/jpestics.D17-094

Table 2. NMR data of 2 (DMSO-d6) and 2′ (CDCl3).

Position 2 2
δH (J in Hz) δC δH (J in Hz) δC
1 119.0 124.8
2 6.56 d (1.6) 107.6 6.82 d (1.9) 108.9
3 145.6 151.2
4 140.0 142.1
5 148.1 153.2
6 7.19 d (1.6) 107.1 7.30 d (1.9) 107.4
7 166.7 166.5
7-COOH 12.74 brsa)
7-COOMe 3.80 s 52.1
5-OCH3 3.84 s 48.6 3.93 s 56.28
4-OH 9.62 brs
4-OCH3 4.04 s 61.0
1′ 134.8 135.9
2′,6′ 152.7 153.0
3′,5′ 7.36 s 106.6 7.37 s 106.8
4′ 128.2 127.3
7′ 166.9 166.8
7′-COOH 12.74 brsa)
7′-COOMe 3.95 s 52.4
2′,6′-OCH3 3.77 s 56.2 3.82 s 56.30

a) Overlapping signals.