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. 2016 May 20;41(2):49–54. doi: 10.1584/jpestics.D15-071

Table 2. Validation parameters of the developed method.

Parameter Pods Leaves Criteriab)
Linearity (r2) 0.999 0.997 ND
Repeatability (RSD %) 3.75 5.43 ≤ 20%
LOD (µg/kg) 0.83 2.7 ND
LOQ (µg/kg) 2.5 8.2 ≤ MRL
Accuracya) (%) 109.38 108.5 70–120%

r2 determination coefficient; LOD limit of detection was calculated as 3 : 1 S/N ratio; LOQ limit of quantification was calculated as 10 : 1 S/N ratio from calibration measurements. a) Accuracy was calculated as the average recovery from all spike levels. b) European Commission requirements (SANCO Document 12571, 2013), unless not determined ND.