Table 1.
Other known dialcarbs and their dissociation temperature [8].
R1 | R2 | mp range (°C) | Dissociation temperature (°C) | bp amine (°C) |
Me | Me | 30-45 | 60-61 | 7.4 |
Me | Et | - | 62 | 34-35 |
Et | Et | 17-33 | 62-63 | 55 |
Me | n-Pr | - | 70-71 | 62 |
-(CH2)4- | - | 55-80 | 105 | 87-88 |
-(CH2)5- | - | 48-63 | - | 106 |
Me | H | 99-133 | - | -6.5 |