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. 2005 Nov 30;10(11):1409–1412. doi: 10.3390/10111409

Table 1.

Comparison between methods, times, temperatures and yields.

Method Reaction Time (min) Temperature (oC)[a] Yield (%)
Microwave irradiation 6-8 266-280 70-85
Sealed tube 1440 120 81
General refluxing 2880 120 84

[a]: Measured by infrared thermometry.