Skip to main content
. 2005 Feb 28;10(2):481–487. doi: 10.3390/10020481

Table 1.

Influence of solvent on yield in final product a

Experiment. Solvent Temperature (°C) Yield (%) b
1 DMSO 160-170 35
2 DMF 140-150 27
3 HMPTA 160-170 21
4 NMP 180-190 80

a) Experiments were performed on the reaction system corresponding to cinnamic acid 3a (see Scheme 1)

b) After recrystallization