Table 2.

Crystal data and structure refinement details

Empirical formula	C26H32Cl8N2O2PdS4	Density (calculated)	1.658 g/mL
Formula weight	922.78	Absorption coefficient	1.334 mm-1
Temperature	100(2) K	F(000)	928
Wavelength	0.71073 Å	Crystal size	0.25 x 0.08 x 0.08 mm3
Crystal system	Monoclinic	θ range for data collection	2.53 to 28.29°
Space group	P2(1)/c	Reflections collected	13380
Unit cell dimensions	a = 18.0079(15) Å, α= 90°	Independent reflections	4358 [R(int) = 0.0367]
	b = 6.0692(5) Å, β= 116.5450(10)°	Final R indices [I>2sigma(I)]	R1 = 0.0364, wR2 = 0.0811
	c = 18.9080(16) Å, γ= 90°	Goodness-of-fit on F2	1.051
Volume	1848.7(3) Å3	R indices (all data)	R1 = 0.0494, wR2 = 0.0862
Z	2	Largest diff. peak and hole	1.350 and -0.811 e.Å-3