Skip to main content
. 2007 Mar 21;12(3):582–592. doi: 10.3390/12030582

Table 1.

1H- and 13C-NMR data of compounds 1 and 2 (500/125 MHz, respectively, in CDCl3; δ in ppm, J in Hz).

No. Compound 1 Compound 2
C H C H
1 141.3 s 137.9 s
2 131.6 s 132.2 s
21 12.1 q 3.47 s 17.1 q 3.64 s
3 136.3 s 139.9 s
31 129.0 d 8.02 dd 11.5, 17.5 129.5 d 8.00 dd 11.5, 17.5
32 122.7 t 6.20 dd 2.3, 17.5
6.36 dd 2.3, 11.5
125.0 t 6.22 dd 2.3, 17.5
6.34 dd 2.3, 11.5
4 135.1 s 133.7 s
5 99.5 s 9.55 s 99.9 d 9.72 s
6 156.0 s 154.1 s
7 136.1 s 137.3 s
71 11.3 q 3.29 s 11.3 q 3.32 s
8 145.5 s 144.9 s
81 19.6 t 3.76 q 7.0 19.5 t 3.77 q 7.0
82 17.6 q 1.73 t 7.0 17.4 q 1.74 t 7.0
9 150.0 s 152.1 s
10 104.1 d 9.78 s 103.8 d 9.72 s
11 139.1 s 139.5 s
12 131.4 s 131.0 s
121 12.5 q 3.94 s 12.4 q 3.78 s
13 112.2 s 128.1 s
131 161.4 s 191.8 s
132 89.3 s
133 172.8 s
14 136.3 s 149.0 s
15 101.5 s 108.3 s
151 106.3 s
152 169.1 s
16 167.8 s 162.9 s
17 53.9 d 4.82 d 7.0 51.8 d 4.20 d 7.5
171 32.2 t 1.90 m; 2.62 m 31.6 t 1.92 m; 2.60 m
172 32.5 t 2.21 m; 2.48 m 30.8 t 2.20 m; 2.46 m
173 173.2 s 173.5 s
18 50.0 d 4.45 q 7.0 50.0 d 4.89 q 7.0
181 22.6 q 1.62 d 7.0 19.7 q 1.50 d 7.0
19 171.8 s 171.2 s
20 94.0 d 8.75 s 106.4s
1’ 61.3 t 4.43 d 7.0 61.6 t 4.62 d 7.0
2’ 117.8 d 5.16 t 7.0 117.8 d 5.26 t 7.0
3’ 142.6 s 142.8 s
4’ 39.8 t 1.90 m 39.8 t 1.88 m
5’ 24.8 t 1.60 m; 1.72 m 24.8 t 1.62 m; 1.70 m
6’ 36.6 t 1.00 m; 1.20 m 36.6 t 1.00 m; 1.20 m
7’ 32.6 d 1.30 m 32.6 d 1.32 m
8’ 37.4 t 1.03 m; 1.26 m 37.3 t 1.03 m; 1.26 m
9’ 24.8 1.28 m 25.0 t 1.28 m
10’ 36.7 t 1.26 m 37.3 t 1.26 m
11’ 32.6 d 1.30 m 32.8 d 1.30 m; 1.26 m
12’ 37.3 t 1.03 m; 1.26 m 37.2 t 1.03 m; 1.26 m
13’ 24.4 t 1.60 m 24.4 t 1.60 m
14’ 39.4 t 1.15 m 39.3 t 1.15 m
15’ 28.0 d 1.51 m 27.9 d 1.50 m
16’ 22.7 q 0.87 d 6.8 22.7 q 0.87 d 6.8
17’ 22.6 q 0.87 d 6.8 22.6 q 0.87 d 6.8
18’ 16.2 q 1.56 s 16.3 q 1.66 s
19’ 19.6 q 0.76 d 6.5 19.6 q 0.84 d 6.5
20’ 19.7 q 0.82 d 6.5 19.7 q 0.83 d 6.5