Table 1.
No. | Compound 1 | Compound 2 | ||
---|---|---|---|---|
C | H | C | H | |
1 | 141.3 s | 137.9 s | ||
2 | 131.6 s | 132.2 s | ||
21 | 12.1 q | 3.47 s | 17.1 q | 3.64 s |
3 | 136.3 s | 139.9 s | ||
31 | 129.0 d | 8.02 dd 11.5, 17.5 | 129.5 d | 8.00 dd 11.5, 17.5 |
32 | 122.7 t | 6.20 dd 2.3, 17.5 6.36 dd 2.3, 11.5 |
125.0 t | 6.22 dd 2.3, 17.5 6.34 dd 2.3, 11.5 |
4 | 135.1 s | 133.7 s | ||
5 | 99.5 s | 9.55 s | 99.9 d | 9.72 s |
6 | 156.0 s | 154.1 s | ||
7 | 136.1 s | 137.3 s | ||
71 | 11.3 q | 3.29 s | 11.3 q | 3.32 s |
8 | 145.5 s | 144.9 s | ||
81 | 19.6 t | 3.76 q 7.0 | 19.5 t | 3.77 q 7.0 |
82 | 17.6 q | 1.73 t 7.0 | 17.4 q | 1.74 t 7.0 |
9 | 150.0 s | 152.1 s | ||
10 | 104.1 d | 9.78 s | 103.8 d | 9.72 s |
11 | 139.1 s | 139.5 s | ||
12 | 131.4 s | 131.0 s | ||
121 | 12.5 q | 3.94 s | 12.4 q | 3.78 s |
13 | 112.2 s | 128.1 s | ||
131 | 161.4 s | 191.8 s | ||
132 | 89.3 s | |||
133 | 172.8 s | |||
14 | 136.3 s | 149.0 s | ||
15 | 101.5 s | 108.3 s | ||
151 | 106.3 s | |||
152 | 169.1 s | |||
16 | 167.8 s | 162.9 s | ||
17 | 53.9 d | 4.82 d 7.0 | 51.8 d | 4.20 d 7.5 |
171 | 32.2 t | 1.90 m; 2.62 m | 31.6 t | 1.92 m; 2.60 m |
172 | 32.5 t | 2.21 m; 2.48 m | 30.8 t | 2.20 m; 2.46 m |
173 | 173.2 s | 173.5 s | ||
18 | 50.0 d | 4.45 q 7.0 | 50.0 d | 4.89 q 7.0 |
181 | 22.6 q | 1.62 d 7.0 | 19.7 q | 1.50 d 7.0 |
19 | 171.8 s | 171.2 s | ||
20 | 94.0 d | 8.75 s | 106.4s | |
1’ | 61.3 t | 4.43 d 7.0 | 61.6 t | 4.62 d 7.0 |
2’ | 117.8 d | 5.16 t 7.0 | 117.8 d | 5.26 t 7.0 |
3’ | 142.6 s | 142.8 s | ||
4’ | 39.8 t | 1.90 m | 39.8 t | 1.88 m |
5’ | 24.8 t | 1.60 m; 1.72 m | 24.8 t | 1.62 m; 1.70 m |
6’ | 36.6 t | 1.00 m; 1.20 m | 36.6 t | 1.00 m; 1.20 m |
7’ | 32.6 d | 1.30 m | 32.6 d | 1.32 m |
8’ | 37.4 t | 1.03 m; 1.26 m | 37.3 t | 1.03 m; 1.26 m |
9’ | 24.8 | 1.28 m | 25.0 t | 1.28 m |
10’ | 36.7 t | 1.26 m | 37.3 t | 1.26 m |
11’ | 32.6 d | 1.30 m | 32.8 d | 1.30 m; 1.26 m |
12’ | 37.3 t | 1.03 m; 1.26 m | 37.2 t | 1.03 m; 1.26 m |
13’ | 24.4 t | 1.60 m | 24.4 t | 1.60 m |
14’ | 39.4 t | 1.15 m | 39.3 t | 1.15 m |
15’ | 28.0 d | 1.51 m | 27.9 d | 1.50 m |
16’ | 22.7 q | 0.87 d 6.8 | 22.7 q | 0.87 d 6.8 |
17’ | 22.6 q | 0.87 d 6.8 | 22.6 q | 0.87 d 6.8 |
18’ | 16.2 q | 1.56 s | 16.3 q | 1.66 s |
19’ | 19.6 q | 0.76 d 6.5 | 19.6 q | 0.84 d 6.5 |
20’ | 19.7 q | 0.82 d 6.5 | 19.7 q | 0.83 d 6.5 |