Table 1.
Cd. 1 | Cd. 2 | Cd. 3 | Cd. 4 | Cd. 5 | Cd. 6 | Cd. 7 | |
---|---|---|---|---|---|---|---|
Yield (%) | 53.2 | 48.3 | 45.1 | 65.3 | 41.3 | 66.3 | 69.6 |
Color | White powder | White powder | Yellow needle crystal | White needle crystal | Yellow powder | While needle crystal | Light yellow powder |
m.p. (°C) | >244 a | 180–181 | 229–230 | 164–165 | >200 a | 162–163 | 178–180 |
ESI-MS (m/z) | 238.05 b | 250.08 c | 264.07 c | 292.3 c | 286.2 c | 318.3 c | 312.3 c |
a Decomposing temperature; b [M + 1]+; c [M − 1]−.