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. 2017 Sep 10;22(9):1517. doi: 10.3390/molecules22091517

Table 5.

The determination results of Orlistat by qNMR and HPLC.

Batch No. qNMR (n = 3) HPLC
δ % Label Claim RSD% % Label Claim RSD%
15082101 5.64 100.65 0.38 99.71 0.61
8.94 99.99 0.34
21606151 5.64 98.58 1.11 96.75 0.85
8.94 99.03 0.86
21605111 5.64 98.75 0.33 97.87 1.20
8.94 97.42 0.51

*δ in ppm.