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. 2017 Sep 1;22(9):1454. doi: 10.3390/molecules22091454

Table 1.

1H- and 13C-NMR spectral data of 1 (CD3OD, 400 MHz).

Position δH (mult., J in Hz) δC
1 168.2
2 5.79 (1H, s) 118.3
3 152.0
4 8.00 (1H, d, 15.7) 131.7
5 6.55 (1H, d, 15.7) 135.7
1′ 83.3
2′ 87.8
3′ 2.03 (1H, dd, 13.7, 7.0) 1.73 (1H, dd, 13.7, 10.4) 46.0
4′ 4.12 (1H, m) 66.0
5′ 1.86 (1H, dd, 13.5, 6.9) 1.68 (1H, dd, 13.5, 13.5) 44.6
6′ 49.2
7′ 1.16 (3H, s) 19.6
8′ 0.94 (3H, s) 16.4
9′ 3.82 (1H, d, 7.5) 3.72 (1H, d, 7.5) 77.3
CH3-3 2.10 (3H, s,) 21.2
OCH3 3.70 (3H, s) 51.6