Table 1.
Position | δC | δH (J in Hz) | HMBC |
---|---|---|---|
1 | 130.3 | ||
2 | 112.5 | 7.56, d, 2.0 | C-1, C-3, C-4, C-6, C=O |
3 | 149.0 | C-1, C-2, C-4, C-5 | |
4 | 153.3 | ||
5 | 115.7 | 6.80, d, 8.5 | C-1, C-3, C-4, C-6 |
6 | 125.2 | 7.62, dd, 8.5, 2.0 | C-1, C-2, C-4, C-5 |
C=O | 199.6 | ||
α | 65.5 | 4.26, dd, 11.0, 8.5, 3.71, dd, 11.0, 5.5 |
C-1, C-1′, C=O, C-β |
β | 56.3 | 4.76, dd, 8.5, 5.0 | C-1′,C-2′, C-6′, C=O, C-α |
1′ | 129.9 | C-α, C-β, C-2′, C-3′, C-5′, C-6′ | |
2′ | 112.7 | 6.89, d, 2.0 | C-β, C-1′,C-3′, C-4′, C-6′ |
3′ | 149.3 | ||
4′ | 147.0 | ||
5′ | 116.6 | 6.73, d, 8.5 | C-1′, C-3′, C-4′, C-6′ |
6′ | 122.2 | 6.76, dd, 8.5, 2.0 | C-β, C-1′,C-2′, C-4′, C-5′ |
3-OCH3 | 56.3 | 3.86, s | C-3 |
4′-OCH3 | 56.4 | 3.82, s | C-4′ |