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. 2017 Aug 25;22(9):1413. doi: 10.3390/molecules22091413

Table 1.

1H-NMR and 13C-NMR data of 1 (600/150 MHz, Methanol-d4).

Position δC δH (J in Hz) HMBC
1 130.3
2 112.5 7.56, d, 2.0 C-1, C-3, C-4, C-6, C=O
3 149.0 C-1, C-2, C-4, C-5
4 153.3
5 115.7 6.80, d, 8.5 C-1, C-3, C-4, C-6
6 125.2 7.62, dd, 8.5, 2.0 C-1, C-2, C-4, C-5
C=O 199.6
α 65.5 4.26, dd, 11.0, 8.5,
3.71, dd, 11.0, 5.5
C-1, C-1′, C=O, C-β
β 56.3 4.76, dd, 8.5, 5.0 C-1′,C-2′, C-6′, C=O, C-α
1′ 129.9 C-α, C-β, C-2′, C-3′, C-5′, C-6′
2′ 112.7 6.89, d, 2.0 C-β, C-1′,C-3′, C-4′, C-6′
3′ 149.3
4′ 147.0
5′ 116.6 6.73, d, 8.5 C-1′, C-3′, C-4′, C-6′
6′ 122.2 6.76, dd, 8.5, 2.0 C-β, C-1′,C-2′, C-4′, C-5′
3-OCH3 56.3 3.86, s C-3
4′-OCH3 56.4 3.82, s C-4′