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. 2017 Jul 21;22(7):1231. doi: 10.3390/molecules22071231

Table 3.

The relative retention times and characteristic peak areas of each AD sample measured by HPLC (3).

No. S23 S24 S25 S26 S27 S28 S29 S30 S31 S32
Retention Time (min) 31.563 32.423 34.010 34.539 38.207 40.534 44.779 46.637 48.727 49.215
Crude AD 560,224.6 972,543.3 324,065.4 12,375.4 15,736.7 79,450.6 38,132.1 221,740.0 74,890.7 53,851.1
50 °C-54 h 592,867.9 952,622.1 359,651.1 9959.8 12,801.1 50,618.0 15,379.2 194,528.8 76,754.9 55,754.0
50 °C-108 h 523,442.3 671,940.9 206,552.5 6730.8 12,304.7 32,556.7 7312.1 125,685.2 38,401.4 35,661.4
50 °C-162 h 547,212.2 798,756.6 297,107.3 12,310.5 10,733.5 50,606.9 7524.8 147,790.4 61,352.6 49,594.6
50 °C-216 h 698,967.6 791,620.5 237,683.6 6392.9 15,180.0 41,922.0 4493.3 138,720.0 53,250.9 36,872.8
60 °C-18 h 598,011.3 817,165.9 226,284.2 4002.6 16,522.4 43,831.0 5371.3 146,085.0 53,376.8 35,968.6
60 °C-36 h 671,001.0 1,559,512.0 517,576.6 7811.5 15,443.2 49,068.4 14,457.4 252,143.1 154,725.1 76,879.2
60 °C-54 h 550,049.8 696,035.7 191,708.6 8854.8 9577.9 59,635.0 4772.7 117,058.2 49,246.5 30,484.4
60 °C-72 h 684,153.5 1,022,686.0 319,185.7 8,420.6 16,577.5 96,335.4 8999.1 185,007.3 87,662.8 51,117.9
70 °C-6 h 888,239.6 1,149,116.0 356,770.1 45,253.0 14,881.3 59,347.8 20,490.8 254,956.0 103,836.8 53,336.2
70 °C-12 h 515,345.2 1,038,435.0 324,011.2 3870.5 12,361.4 70,781.8 7478.0 143,041.9 76,715.8 45,315.0
70 °C-18 h 515,812.7 855,437.6 226,695.7 12,388.8 13,938.8 63,813.1 7266.0 142,116.2 55,039.4 33,938.2
70 °C-24 h 528,147.1 717,764.8 242,327.2 7423.3 10,147.6 52,933.8 7588.3 129,583.3 50,142.5 38,381.5
80 °C-2 h 529,400.1 1,081,962.0 331,856.6 16,461.1 16,206.7 79,560.9 8972.2 235,615.9 81,353.9 45,462.3
80 °C-4 h 481,003.8 715,983.4 211,356.3 4006.6 10,224.1 70,918.2 8020.7 118,561.2 37,647.7 31,555.4
80 °C-6 h 493,469.0 959,465.1 289,452.9 7777.3 10,934.7 55,410.2 9575.2 134,500.4 68,113.8 45,316.9
80 °C-8 h 514,575.9 714,618.2 174,512.4 8516.8 12,392.8 57,624.0 6510.2 109,653.8 54,442.2 28,237.6