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. 2017 Jul 21;22(7):1231. doi: 10.3390/molecules22071231

Table 4.

The relative retention times and characteristic peak areas of each AD sample measured by HPLC (4).

No. S33 S34 S35 S36 S37 S38 S39 S40 S41 S42
Retention Time (min) 52.975 57.024 57.712 59.902 61.564 63.915 69.301 73.914 80.610 86.761
Crude AD 50,927.6 104,182.2 98,552.5 15,237.1 223,590.3 129,231.9 39,349.3 233,160.5 163,906.4 80,309.9
50 °C-54 h 61,884.9 121,212.5 77,736.0 15,603.0 173,632.8 108,427.6 28,718.7 169,335.6 171,291.8 68,429.0
50 °C-108 h 50,695.9 77,357.7 81,845.5 6325.0 196,267.5 95,585.5 29,278.7 150,975.6 107,235.6 39,845.1
50 °C-162 h 57,769.9 99,849.1 69,414.0 11,536.5 163,271.2 95,884.5 26,292.0 125,074.5 127,355.6 45,658.7
50 °C-216 h 52,017.2 86,033.1 81,737.7 6161.6 196,815.6 79,059.4 23,188.8 102,873.3 79,174.49 23,643.8
60 °C-18 h 55,377.1 76,850.4 106,775.5 13,403.5 249,757.4 120,852.6 35,528.9 147,422.0 113,002.2 32,847.6
60 °C-36 h 46,064.2 168,804.0 66,507.5 20,226.8 158,937.3 110,019.5 31,767.1 126,495.3 103,918.3 66,471.0
60 °C-54 h 66,850.1 66,097.1 96,060.6 8898.1 210,225.6 104,151.9 29,404.0 137,078.3 142,889.0 38,094.2
60 °C-72 h 64,494.1 116,323.1 104,203.6 5167.0 237,645.0 103,592.8 29,812.4 167,396.3 128,140.2 45,190.8
70 °C-6 h 94,353.5 126,491.1 76,047.4 20,075.6 157,759.3 99,033.5 25,914.1 158,990.7 212,661.6 68,108.6
70 °C-12 h 54,847.3 97,420.0 71,124.9 9211.7 149,427.0 104,972.3 28,759.3 127,258.2 121,153.1 60,246.6
70 °C-18 h 69,949.1 80,301.0 122,020.0 8565.0 265,616.2 126,703.1 37,832.2 217,166.1 166,001.8 52,442.1
70 °C-24 h 46,707.2 81,846.3 65,079.2 8844.5 152,320.3 82,649.1 22,604.9 99,800.0 82,473.0 36,173.8
80 °C-2 h 60,933.6 100,513.7 74,468.1 21,270.0 155,195.0 111,084.7 30,547.7 142,233.2 142,818.2 52,632.0
80 °C-4 h 60,916.4 67,297.8 84,519.6 10,242.4 172,952.2 97,036.15 26,573.2 145,393.5 139,343.8 41,105.5
80 °C-6 h 56,125.2 94,188.2 90,992.7 9866.5 205,797.5 125,516.2 36,502.4 160,414.3 127,849.3 51,528.5
80 °C-8 h 58,813.7 72,510.2 108,250.4 17,090.3 241,306.9 99,497.3 30,808.6 178,600.2 138,638.6 41,439.8