Table 3.
Recovery of Five FAs in Samples.
| Compound | Initial(mg) | Amount(mg) | Add(mg) | Found ± SD(mg) | Recovery (%) | RSD (%, n = 3) |
|---|---|---|---|---|---|---|
| Linolenic acid | 8.87 | 0.0177 | 0.0089 | 0.0265 ± 0.0006 | 98.30 | 2.79 |
| 8.96 | 0.0179 | 0.0090 | 0.0272 ± 0.0002 | 103.68 | ||
| 8.71 | 0.0174 | 0.0087 | 0.0264 ± 0.0003 | 102.55 | ||
| 8.48 | 0.0170 | 0.0170 | 0.0331 ± 0.0005 | 95.19 | 2.17 | |
| 8.71 | 0.0174 | 0.0174 | 0.0346 ± 0.0005 | 98.65 | ||
| 8.63 | 0.0173 | 0.0173 | 0.0336 ± 0.0006 | 94.91 | ||
| 8.11 | 0.0162 | 0.0243 | 0.0398 ± 0.0006 | 96.71 | 2.20 | |
| 8.04 | 0.0161 | 0.0241 | 0.0404 ± 0.0004 | 101.03 | ||
| 8.23 | 0.0165 | 0.0247 | 0.0408 ± 0.0004 | 98.46 | ||
| Linoleic acid | 8.87 | 1.2306 | 0.6153 | 1.8451 ± 0.0116 | 99.87 | 2.66 |
| 8.96 | 1.2431 | 0.6216 | 1.8414 ± 0.0037 | 96.25 | ||
| 8.71 | 1.2084 | 0.6042 | 1.7817 ± 0.0133 | 94.88 | ||
| 8.48 | 1.1765 | 1.1765 | 2.3642 ± 0.0061 | 100.95 | 2.21 | |
| 8.71 | 1.2084 | 1.2084 | 2.4752 ± 0.0070 | 104.83 | ||
| 8.63 | 1.1973 | 1.1973 | 2.4545 ± 0.0041 | 105.00 | ||
| 8.11 | 11252 | 1.6878 | 2.8308 ± 0.0307 | 101.06 | 1.84 | |
| 8.04 | 1.1155 | 1.6732 | 2.8386 ± 0.0064 | 102.98 | ||
| 8.23 | 1.1418 | 1.7127 | 2.9375 ± 0.1431 | 104.84 | ||
| Palmitic acid | 8.87 | 0.6905 | 0.3453 | 1.0414 ± 0.0146 | 101.63 | 1.49 |
| 8.96 | 0.6975 | 0.3478 | 1.0604 ± 0.0014 | 104.03 | ||
| 8.71 | 0.6781 | 0.3390 | 1.0212 ± 0.0005 | 101.21 | ||
| 8.48 | 0.6602 | 0.6602 | 1.2946 ± 0.0044 | 96.10 | 1.82 | |
| 8.71 | 0.6781 | 0.6781 | 1.3456 ± 0.0027 | 98.44 | ||
| 8.63 | 0.6718 | 0.6718 | 1.3411 ± 0.0080 | 99.62 | ||
| 8.11 | 0.6314 | 0.9470 | 1.6031 ± 0.0235 | 102.60 | 0.94 | |
| 8.04 | 0.6259 | 0.9389 | 1.6065 ± 0.0033 | 104.44 | ||
| 8.23 | 0.6407 | 0.9611 | 1.6301 ±0.0197 | 102.94 | ||
| Oleic acid | 8.87 | 2.9146 | 1.4573 | 4.3238 ± 0.0055 | 96.70 | 2.71 |
| 8.96 | 2,9442 | 1.4721 | 4.4206 ± 0.0068 | 100.29 | ||
| 8.71 | 2.8620 | 1.4310 | 4.3215 ± 0.0102 | 101.99 | ||
| 8.48 | 2.7864 | 2.7864 | 5.4940 ± 0.0036 | 97.17 | 1.15 | |
| 8.71 | 2.8620 | 2.8620 | 5.6369 ± 0.0138 | 96.96 | ||
| 8.63 | 2.8357 | 2.8357 | 5.5337 ± 0.0057 | 95.14 | ||
| 8.11 | 2.6649 | 3.9973 | 6.6010 ± 0.0695 | 98.47 | 1.29 | |
| 8.04 | 2.6419 | 3.9628 | 6.6026 ± 0.0303 | 99.95 | ||
| 8.23 | 2.7043 | 4.0564 | 6.8029 ± 0.3343 | 101.04 | ||
| Stearic acid | 8.87 | 0.3869 | 0.1930 | 0.5709 ± 0.0018 | 95.80 | 2.94 |
| 8.96 | 0.3899 | 0.1950 | 0.5799 ± 0.0020 | 97.42 | ||
| 8.71 | 0.3791 | 0.1896 | 0.5713 ± 0.0036 | 101.41 | ||
| 8.48 | 0.3690 | 0.3690 | 0.7205 ± 0.0037 | 95.24 | 2.33 | |
| 8.71 | 0.3791 | 0.3791 | 0.7566 ± 0.0038 | 99.60 | ||
| 8.63 | 0.3756 | 0.3756 | 0.7376 ± 0.0109 | 96.38 | ||
| 8.11 | 0.3529 | 0.5294 | 0.8560 ± 0.0113 | 95.03 | 1.19 | |
| 8.04 | 0.3499 | 0.5249 | 0.8498 ± 0.0070 | 95.24 | ||
| 8.23 | 0.3582 | 0.5373 | 0.8799 ± 0.0062 | 97.10 |