Table 1.
Ring | No. | 13C | 1H | Ring | No. | 13C | 1H | Ring | No | 13C | 1H |
---|---|---|---|---|---|---|---|---|---|---|---|
C | 2 | 79.01 | 5.7, s, m | C′ | 2′ | 105.08 | 3.28 (d, 3.47) 4.15 (d, 3.47) |
C″ | 2″ | 80.44 | 4.39 (s) |
3 | 72.72 | 4.13, d, m | 3′ | 67.33 | 3.28 (d, 3.47) | 3″ | 67.67 | 3.87–3.85 (m) | |||
4 | 38.92 | 4.6, br, s | 4′ | 29.01 | 4.15, (d, 3.47) | 4″ | 30 | a. 2.84 (dd, 4.6, 17.3) b. 2.84 (dd, 4.6, 17.3) |
|||
A | 5 | 156.90 | A′ | 5′ | 151.2 | A″ | 5″ | 156.16 | |||
6 | 98.9 | 6.02 (d, 2.3) | 6′ | 96.21 | 5.8 (s) | 6″ | 96.61 | 6.10 (s) | |||
7 | 157.95 | 7′ | 155.9 | 7″ | 155.94 | ||||||
8 | 96.7 | 5.98 (d, 2.3) | 8′ | 106.87 | 8″ | 108.9 | |||||
9 | 154.29 | 9′ | 151.92 | 9″ | 151.92 | ||||||
10 | 106.55 | 10′ | 100.09 | 10″ | 100.19 | ||||||
B | 11 | 131 | B′ | 11′ | 119.56 | B″ | 11″ | 133.3 | |||
12 | 116.86 | 7.32 d (1.9) | 12′ | 115.88 | 6.10 d (1.5) | 12″ | 115.85 | 7.03 (d, 1.93) | |||
13 | 145.89 | 13′ | 145.46 | 13″ | 146.74 | ||||||
14 | 146.42 | 14′ | 145.89 | 14″ | 146.03 | ||||||
15 | 120.01 | 6.83 (d, 8.0) | 15′ | 116.14 | 6.83 (d, 8.0) | 15″ | 116.27 | 6.75 (d, 8.0) | |||
16 | 121.49 | 7.2 (dd, 1.9, 8) | 16′ | 115.61 | 7.2 (dd, 1.9, 8) | 16″ | 119.56 | 6.73 (dd, 1.93, 8.04) |