Table 2.
Fractions and Combined Eluates * | Elution Volume (mL) ** | Yield (g) | Isolated Compounds |
---|---|---|---|
I-VIII 1–540 | 4455 | 0.71977 | |
IX 541–550 | 200 | 0.0921 | |
X 551–565 | 320 | 0.1638 | |
XI 566–585 | 300 | 0.0801 | |
XII 586–625 | 670 | 0.3187 | |
XIII 626–660 | 530 | 0.4814 | |
XIV 661–690 | 410 | 0.2181 | |
XV 691–720 | 370 | 0.1548 | 2, 3, 4 |
XVI 721–819 | 1020 | 0.3595 | |
XVII 820–890 | 980 | 0.2426 | |
XVIII 891–909 | 330 | 0.0696 | |
XIX 910–940 | 510 | 0.1803 | 1 |
XX 941–1010 | 760 | 0.3141 | 1, 5, 6 |
XXI 1011–1080 | 840 | 0.5080 | |
XXII 1081–1140 | 850 | 0.5072 | 8, 9, 10 |
XXIII 1141–1200 | 710 | 0.1973 | |
XXIV 1201–1210 | 83 | 0.0244 | |
XXV 1211–1225 | 120 | 0.0381 | |
XXVI 1226–1280 | 490 | 0.1175 | |
XXVII 1281–1319 | 340 | 0.0619 | |
XXVIII 1320–1335 | 230 | 0.0493 | |
XXIX 1336–1380 | 780 | 0.1580 | |
XXX 1381–1410 | 480 | 0.1136 | |
XXXI 1411–1470 | 950 | 0.1796 | |
XXXII 1471–1750 | 4420 | 0.5834 | |
XXXIII 1751–1830 | 1230 | 0.0782 | |
XXXIV 1831–1875 | 540 | 0.0508 | |
XXXV 1876–1885 | 80 | 0.7643 | |
XXXVI 1886–1919 | 520 | 0.3215 | |
XXXVII 1920–1959 | 800 | 0.1256 | |
XXXVIII 1960–2023 | 1080 | 0.1762 | |
Total: | Total: | ||
25,398 | 7.4498 |
* tube 1–459: 10 mL; tube 460–2023: 20 mL; ** eluate amounts determined volumetrically.