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. 2017 May 6;22(5):747. doi: 10.3390/molecules22050747

Table 2.

13C-NMR spectroscopic data (CDCl3) for compounds 14.

Position 1 3 4 2 a
δC Mult. δC Mult. δC Mult. δC Mult.
1 182.80 s 184.75 s 197.20 s 196.91 s
2 158.31 s 144.36 s 135.84 s 137.29 s
3 107.09 s 144.21 s 160.58 s 158.20 s
4 186.95 s 183.90 s 67.88 d 69.10 d
5 138.75 s 138.85 s 43.40 d 43.00 d
6 144.09 s 141.67 s 40.24 d 41.29 d
7 25.68 t 25.29 t 26.94 t 26.84 t
8 118.98 d 118.87 d 121.19 d 120.36 d
9 137.51 s 137.57 s 137.76 s 137.77 s
10 39.68 t 39.68 t 39.62 t 39.60 t
11 26.43 t 26.45 t 26.35 t 26.44 t
12 123.82 d 123.83 d 124.83 d 124.90 d
13 135.19 s 135.18 s 134.04 s 133.80 s
14 39.66 t 39.67 t 42.20 t 42.29 t
15 26.74 d 26.72 d 125.22 d 125.26 d
16 124.30 d 124.29 d 139.16 d 139.20 d
17 131.29 s 131.27 s 70.76 s 70.63 s
18 25.48 q 25.67 q 29.85 q 29.77 q
19 17.65 q 17.64 q 29.80 q 29.77 q
20 16.00 q 15.98 q 16.14 q 16.02 q
21 16.34 q 16.30 q 16.14 q 16.08 q
22 11.85 q 11.92 s 12.32 q 12.83 q
23 56.07 q 61.12 q 60.59 q 60.69 q
24 61.12 q 59.20 q 59.67 q

a Acetate group: δ 169.77 (s, C=O), 20.94 (q, CH3).