Table 2.
Position | 1 | 3 | 4 | 2 a |
---|---|---|---|---|
δC Mult. | δC Mult. | δC Mult. | δC Mult. | |
1 | 182.80 s | 184.75 s | 197.20 s | 196.91 s |
2 | 158.31 s | 144.36 s | 135.84 s | 137.29 s |
3 | 107.09 s | 144.21 s | 160.58 s | 158.20 s |
4 | 186.95 s | 183.90 s | 67.88 d | 69.10 d |
5 | 138.75 s | 138.85 s | 43.40 d | 43.00 d |
6 | 144.09 s | 141.67 s | 40.24 d | 41.29 d |
7 | 25.68 t | 25.29 t | 26.94 t | 26.84 t |
8 | 118.98 d | 118.87 d | 121.19 d | 120.36 d |
9 | 137.51 s | 137.57 s | 137.76 s | 137.77 s |
10 | 39.68 t | 39.68 t | 39.62 t | 39.60 t |
11 | 26.43 t | 26.45 t | 26.35 t | 26.44 t |
12 | 123.82 d | 123.83 d | 124.83 d | 124.90 d |
13 | 135.19 s | 135.18 s | 134.04 s | 133.80 s |
14 | 39.66 t | 39.67 t | 42.20 t | 42.29 t |
15 | 26.74 d | 26.72 d | 125.22 d | 125.26 d |
16 | 124.30 d | 124.29 d | 139.16 d | 139.20 d |
17 | 131.29 s | 131.27 s | 70.76 s | 70.63 s |
18 | 25.48 q | 25.67 q | 29.85 q | 29.77 q |
19 | 17.65 q | 17.64 q | 29.80 q | 29.77 q |
20 | 16.00 q | 15.98 q | 16.14 q | 16.02 q |
21 | 16.34 q | 16.30 q | 16.14 q | 16.08 q |
22 | 11.85 q | 11.92 s | 12.32 q | 12.83 q |
23 | 56.07 q | 61.12 q | 60.59 q | 60.69 q |
24 | 61.12 q | 59.20 q | 59.67 q |
a Acetate group: δ 169.77 (s, C=O), 20.94 (q, CH3).