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. 2017 Jan 18;22(1):150. doi: 10.3390/molecules22010150

Table 2.

Heck reaction of aryl halides and n-butyl acrylate catalyzed by OCMCS-Ni a.

graphic file with name molecules-22-00150-i020.jpg

Entry ArX Product Yield b/%
1 graphic file with name molecules-22-00150-i021.jpg graphic file with name molecules-22-00150-i022.jpg 94
2 graphic file with name molecules-22-00150-i023.jpg graphic file with name molecules-22-00150-i024.jpg 86
3 graphic file with name molecules-22-00150-i025.jpg graphic file with name molecules-22-00150-i026.jpg 88
4 graphic file with name molecules-22-00150-i027.jpg graphic file with name molecules-22-00150-i028.jpg 67
5 graphic file with name molecules-22-00150-i029.jpg graphic file with name molecules-22-00150-i030.jpg 79
6 graphic file with name molecules-22-00150-i031.jpg graphic file with name molecules-22-00150-i032.jpg 72
7 graphic file with name molecules-22-00150-i033.jpg graphic file with name molecules-22-00150-i034.jpg 87
8 graphic file with name molecules-22-00150-i035.jpg graphic file with name molecules-22-00150-i036.jpg -
9 graphic file with name molecules-22-00150-i037.jpg graphic file with name molecules-22-00150-i038.jpg -

a Reaction conditions: aryl halides (1.0 mmol), n-butyl acrylate (1.1 mmol); OCMCS-Ni (0.04 mmol Ni), DMF (5.0 mL) at 140 °C for 12.0 h; b The reaction yields were determined by GC-MS analysis of the crude reaction product.