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. 2016 Dec 29;22(1):46. doi: 10.3390/molecules22010046

Table 2.

Details of the X-ray Data Collections and Refinements for Compounds 5, 7, 8 and 9.

	Compound
	5	7	8	9
Formula	C₁₈H₁₇ClN₂Se	C₁₉H₂₀N₂OSe	C₁₉H₂₀N₂Se	C₁₈H₁₇N₃O₂Se
M	375.76	371.34	355.34	386.31
Crystal system	monoclinic	orthorhombic	monoclinic	monoclinic
Space group	P2₁	P2₁2₁2₁	P2₁	P2₁/n
a/Å	10.657(7)	6.6544(8)	10.719(4)	10.5159(7)
b/Å	7.525(5)	7.8134(9)	7.495(3)	7.5401(5)
c/Å	11.320(8)	33.372(4)	11.294(4)	20.9330(15)
α	90	90	90	90
β	115.852(8)	90	115.650(6)	91.879(2)
γ	90	90	90	90
U/A³	817.0(10)	1735.1(4)	818.0(5)	1658.9(2)
Z	2	4	2	4
µ/cm⁻¹	24.591	21.703	22.939	22.793
Reflections collected	7051	11,930	6175	12,160
Independent reflections	2587	3043	1540	2895
R_int	0.0291	0.1535	0.0336	0.0679
R1	0.0249	0.0695	0.0532	0.0394
wR2 [I > 2σ(I)]	0.0544	0.1012	0.1398	0.0903