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Relative retention (k’) of 2-acetylanthracene (10), 9-acetylphenanthrene (14), and the racemic alcohols 15 and 16 derived from each.
| CSP | Analyte | |||
|---|---|---|---|---|
| 10 | 15 Enantiomers | 14 | 16 Enantiomers | |
| “OJ-H” | 96 | 32.4, 95.2 (α = 2.94) | 8.6 | 4.35, 4.68 (α = 1.07) |
| “OD-H” | 4.8 | 2.42, 4.87 (α = 2.01) | 186 | 20.8, 123 (α = 5.88) |
10 and 14 were chromatographed with hexane/2-propanol (100:1 v/v) mixture, and 15 and 16 with hexane/2-propanol (9:1 v/v) mixture. Every k’ was calculated with the V0 value of 3.1 mL.
