Table 4.
Compound No. | Concentration (ng/mL) | Recovery | Matrix Effect | ||
---|---|---|---|---|---|
Accuracy (%) | Precision (RSD, %) | Accuracy (%) | Precision (RSD, %) | ||
1 | 2.82 | 65.08 | 15.97 | 66.75 | 7.21 |
1.41 × 102 | 76.68 | 13.03 | 89.40 | 9.01 | |
2.82 × 103 | 77.94 | 8.93 | 87.77 | 7.89 | |
2 | 2.27 | 75.37 | 10.35 | 74.29 | 8.18 |
1.14 ×102 | 81.09 | 6.13 | 89.13 | 7.66 | |
1.14 ×103 | 88.93 | 9.22 | 91.01 | 7.94 | |
3 | 1.87 | 70.53 | 10.13 | 88.18 | 6.51 |
9.35 × 10 | 81.45 | 9.56 | 90.15 | 9.18 | |
9.35 ×102 | 90.06 | 9.44 | 90.93 | 9.10 | |
4 | 1.77 | 69.97 | 7.07 | 89.37 | 13.95 |
8.85 × 10 | 70.93 | 7.93 | 88.16 | 11.03 | |
1.77 × 103 | 79.83 | 6.54 | 95.43 | 9.75 | |
5 | 1.82 | 71.95 | 11.98 | 89.73 | 10.57 |
9.10 × 10 | 85.54 | 11.99 | 92.05 | 10.66 | |
9.10 × 102 | 89.78 | 10.29 | 95.96 | 8.59 | |
6 | 2.11 | 73.18 | 7.53 | 81.55 | 11.64 |
1.06 × 102 | 89.54 | 8.17 | 88.94 | 10.75 | |
1.06 × 103 | 99.17 | 2.91 | 93.75 | 10.16 | |
7 | 2.22 | 72.34 | 8.93 | 74.58 | 8.15 |
1.11 × 102 | 77.95 | 8.79 | 80.13 | 8.34 | |
2.22 × 103 | 86.76 | 8.10 | 92.22 | 8.03 | |
8 | 2.14 | 81.59 | 11.57 | 78.93 | 7.58 |
1.07 × 102 | 87.63 | 12.63 | 91.54 | 6.85 | |
1.07 × 103 | 103.05 | 11.59 | 99.78 | 11.06 | |
9 | 1.81 | 79.07 | 5.79 | 78.65 | 8.31 |
9.05 × 10 | 81.59 | 8.73 | 82.25 | 7.98 | |
1.81 × 103 | 101.15 | 5.12 | 89.94 | 8.82 | |
10 | 1.85 | 69.34 | 8.57 | 73.54 | 11.13 |
9.25 × 10 | 77.08 | 7.70 | 84.75 | 7.91 | |
9.25 × 102 | 86.45 | 5.94 | 88.63 | 8.54 | |
11 | 1.82 | 83.11 | 8.91 | 84.39 | 15.34 |
9.10 × 10 | 102.53 | 11.35 | 89.15 | 12.68 | |
1.82 × 103 | 100.78 | 7.65 | 103.76 | 5.94 |