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. 2017 Jan 11;22(1):108. doi: 10.3390/molecules22010108

Table 1.

1H (600 MHz) and 13C-NMR (150 MHz) spectroscopic data of compound 6 (CDCl3, δ (ppm), J (Hz)).

Pos. δH δC Pos. δH δC
1 1.57, m 32.6 20 1.99, m 40.4
1.97, m
2 1.41, m 30.7 21 0.95, d, 6.5 21.2
3 4.02, m 67.5 22 5.09, dd, 15.3, 7.7 135.4
4 1.69, m 39.4 23 5.14, dd, 15.3, 7.0 132.2
1.87, m
5 - 75.5 24 1.80, m 42.9
6 4.93, d, 5.4 73.5 25 1.40, m 33.1
7 5.26, d, 5.4 114.3 26 0.76, d, 6.5 20.3
8 - 145.9 27 0.76, d, 6.5 19.7
9 1.94, m 43.4 28 0.84, d, 6.7 17.6
10 - 37.3 1′ - 166.4
11 1.55, m 22.2 2′ 6.33, d, 16.0 118.4
12 1.27, m 39.3 3′ 7.58, d, 16.0 145.1
1.68, m
13 - 43.9 4′ - 134.4
14 1.87, m 55.0 5′ 7.46, d, 8.0 128.2
15 1.35, m 22.8 6′ 7.30–7.31, m 128.9
1.51, m
16 1.21, m 27.9 7′ 7.30–7.31, m 130.4
1.67, m
17 1.22, m 56.0 8′ 7.30–7.31, m 128.9
18 0.53, s 12.5 9′ 7.46, d, 8.0 128.2
19 1.08, s 18.5