Table 1.
Pos. | δH | δC | Pos. | δH | δC |
---|---|---|---|---|---|
1 | 1.57, m | 32.6 | 20 | 1.99, m | 40.4 |
1.97, m | |||||
2 | 1.41, m | 30.7 | 21 | 0.95, d, 6.5 | 21.2 |
3 | 4.02, m | 67.5 | 22 | 5.09, dd, 15.3, 7.7 | 135.4 |
4 | 1.69, m | 39.4 | 23 | 5.14, dd, 15.3, 7.0 | 132.2 |
1.87, m | |||||
5 | - | 75.5 | 24 | 1.80, m | 42.9 |
6 | 4.93, d, 5.4 | 73.5 | 25 | 1.40, m | 33.1 |
7 | 5.26, d, 5.4 | 114.3 | 26 | 0.76, d, 6.5 | 20.3 |
8 | - | 145.9 | 27 | 0.76, d, 6.5 | 19.7 |
9 | 1.94, m | 43.4 | 28 | 0.84, d, 6.7 | 17.6 |
10 | - | 37.3 | 1′ | - | 166.4 |
11 | 1.55, m | 22.2 | 2′ | 6.33, d, 16.0 | 118.4 |
12 | 1.27, m | 39.3 | 3′ | 7.58, d, 16.0 | 145.1 |
1.68, m | |||||
13 | - | 43.9 | 4′ | - | 134.4 |
14 | 1.87, m | 55.0 | 5′ | 7.46, d, 8.0 | 128.2 |
15 | 1.35, m | 22.8 | 6′ | 7.30–7.31, m | 128.9 |
1.51, m | |||||
16 | 1.21, m | 27.9 | 7′ | 7.30–7.31, m | 130.4 |
1.67, m | |||||
17 | 1.22, m | 56.0 | 8′ | 7.30–7.31, m | 128.9 |
18 | 0.53, s | 12.5 | 9′ | 7.46, d, 8.0 | 128.2 |
19 | 1.08, s | 18.5 |