Skip to main content
. Author manuscript; available in PMC: 2019 May 22.
Published in final edited form as: Angew Chem Int Ed Engl. 2018 Apr 26;57(21):6324–6328. doi: 10.1002/anie.201803087

Scheme 1.

Scheme 1.

A) Synthetic route to BDP-NAC. Conditions: i) MgSO4, Et2O, rt, 16 h; ii) AIBN, C6H12, reflux, 16 h; iii) 1) EtOH, rt, 4 h; iv) 1 N NaOH, reflux, 45 min; v) NEt3, CHCl3, rt, 3 h; B) Synthetic route to BDP-Fluor. Conditions: vi) CHCl3:MeOH (1:1 v/v), rt, 40 h.