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. 2018 Sep 28;8:14525. doi: 10.1038/s41598-018-32741-3

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© The Author(s) 2018

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(a) Diagram of the conceptual model of the electrochemical exfoliation process, showing that efficiency of cylindrical electrode exfoliation varies inversely with radius R at large R values. (b) Diagram and (c) picture of prototype batch reactor, with working electrode in an expandable, permeable cylindrical container. (d) Diagram and (e) picture of prototype reactor for forced electrolyte flow through a tileable 2-D graphite electrode with platinized titanium mesh. (f) Schematic for continuous production of EEG in a permeable plug-flow reactor with forced electrolyte flow.