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. Author manuscript; available in PMC: 2018 Oct 15.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2018 Aug 29;1097-1098:35–43. doi: 10.1016/j.jchromb.2018.08.027

Table 1.

Summary of gradient elution profile applied to the chromatographic separation of CLBQ14 and IS from matrix.

Time (min) Flow rate (mL/min) Mobile Phase A (%) Mobile Phase B (%)
0 0.5 80 20
0.8 0.5 30 70
2.8 0.5 5 95
3.8 0.5 5 95
4.0 0.5 60 40
5.5 0.5 60 40