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. 2018 Aug 30;57(38):12742–12755. doi: 10.1021/acs.iecr.8b02678

Table 2. FAME Yield and Productivity Measured in the CCCS at Different Operating Conditions.

exptl run mcat (g) ϕv,oila (mL/min) M WHST (h) wcatb (wt %) τ (min) YFAME (%) PFAME (kgFAME/(m3reactor·h))
1 49.7 12 12 0.075 24.2 18.6 74 757.6
2 33.1 8 9 0.075 14.8 30.4 84 573.4
3 6.6 8 9 0.015 3 30.4 77 525.6
4 49.7 12 6 0.075 20.2 22.2 69 706.4
5 29.8 12 9 0.045 13.3 20.2 76 778.1
6 29.8 12 9 0.045 13.3 20.2 77 788.4
7 29.8 12 9 0.045 13.3 20.2 75 767.9
8 39.7 16 6 0.045 16.2 16.7 65 887.3
9 19.9 8 12 0.045 9.7 27.9 84 573.4
10 9.9 12 6 0.015 4 22.2 66 675.7
11 66.2 16 9 0.075 29.6 15.2 67 914.6
12 39.7 16 12 0.045 19.4 13.9 67 914.6
13 13.2 16 9 0.015 5.9 15.2 62 846.4
14 9.9 12 12 0.015 4.8 18.6 72 737.2
15 29.8 12 9 0.045 13.3 20.2 76 778.1
16 29.8 12 9 0.045 13.3 20.2 77 788.4
17 19.9 8 6 0.045 8.1 33.4 77 525.6
a

In the presence of THF as a cosolvent (5 wt % with repect to the oil).

b

Estimated according to eq 5.