Table 2.
N-Nitrosamine | Spiked level (μg/kg) | Recovery ± SD (%) | Precision (RSD %) | |
---|---|---|---|---|
Intra-day | Inter-day | |||
NDMA | 20 | 108.6 ± 2.26 | 2.08 | 4.22 |
100 | 101.2 ± 0.79 | 0.79 | 3.00 | |
500 | 86.31 ± 1.57 | 1.82 | 6.88 | |
NDEA | 20 | 101.3 ± 0.43 | 0.42 | 2.81 |
100 | 101.7 ± 0.40 | 0.39 | 2.50 | |
500 | 100.1 ± 0.18 | 0.18 | 0.40 | |
NDPA | 20 | 101.0 ± 0.86 | 0.86 | 2.49 |
100 | 101.2 ± 0.50 | 0.50 | 2.32 | |
500 | 101.6 ± 0.18 | 0.18 | 4.86 | |
NDBA | 20 | 104.2 ± 0.59 | 0.59 | 5.51 |
100 | 102.8 ± 0.50 | 0.50 | 1.69 | |
500 | 100.7 ± 0.41 | 0.41 | 0.84 | |
NPIP | 20 | 104.3 ± 0.55 | 0.53 | 2.29 |
100 | 100.2 ± 0.19 | 0.19 | 1.81 | |
500 | 93.70 ± 0.56 | 0.50 | 4.42 | |
NPYR | 20 | 101.8 ± 0.21 | 0.20 | 3.72 |
100 | 100.2 ± 0.64 | 0.64 | 3.08 | |
500 | 93.95 ± 0.57 | 0.61 | 3.41 | |
NMOR | 20 | 102.7 ± 0.25 | 0.24 | 2.64 |
100 | 100.7 ± 0.86 | 0.86 | 1.50 | |
500 | 100.5 ± 0.37 | 0.36 | 0.56 |
All data were calculated from measurements carried out in triplicate