| Rigaku R-AXIS RAPID diffractometer | 1178 reflections with F2 > 2.0σ(F2) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.049 |
| ω scans | θmax = 68.2°, θmin = 4.8° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −8→8 |
| Tmin = 0.543, Tmax = 0.912 | k = −6→7 |
| 4753 measured reflections | l = −22→22 |
| 1566 independent reflections |
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