| Crystal data |
| Chemical formula |
C6H6N2O·H6O6Te |
|
M
r
|
351.8 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c (Å) |
7.0094 (3), 7.5750 (3), 10.6149 (5) |
| α, β, γ (°) |
70.945 (4), 78.748 (4), 89.901 (4) |
|
V (Å3) |
521.32 (4) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.88 |
| Crystal size (mm) |
0.31 × 0.21 × 0.09 |
| |
| Data collection |
| Diffractometer |
Rigaku Oxford Diffraction Xcalibur, AtlasS2, Gemini ultra |
| Absorption correction |
Analytical CrysAlis PRO (Rigaku OD, 2018 ▸) |
|
T
min, T
max
|
0.618, 0.816 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
6995, 2408, 2254 |
|
R
int
|
0.019 |
| (sin θ/λ)max (Å−1) |
0.671 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.012, 0.032, 1.08 |
| No. of reflections |
2408 |
| No. of parameters |
170 |
| No. of restraints |
6 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.42, −0.35 |
