Rigaku XtaLAB mini diffractometer | 4503 independent reflections |
Radiation source: Sealed Tube | 3551 reflections with I > 2σ(I) |
Graphite Monochromator monochromator | Rint = 0.058 |
Detector resolution: 13.6612 pixels mm-1 | θmax = 27.5°, θmin = 2.3° |
profile data from ω–scans | h = −12→12 |
Absorption correction: multi-scan (REQAB; Rigaku, 1998) | k = −13→13 |
Tmin = 0.842, Tmax = 1.00 | l = −14→14 |
10542 measured reflections |