Rigaku XtaLAB mini diffractometer | 4332 independent reflections |
Radiation source: Sealed Tube | 3855 reflections with I > 2σ(I) |
Graphite Monochromator monochromator | Rint = 0.046 |
Detector resolution: 13.6612 pixels mm-1 | θmax = 27.5°, θmin = 2.1° |
profile data from ω–scans | h = −25→25 |
Absorption correction: multi-scan (REQAB; Rigaku, 1998) | k = −13→13 |
Tmin = 0.885, Tmax = 1.00 | l = −24→24 |
19620 measured reflections |