| Rigaku XtaLAB mini diffractometer | 2224 reflections with I > 2σ(I) |
| Detector resolution: 13.6612 pixels mm-1 | Rint = 0.074 |
| profile data from ω–scans | θmax = 27.6°, θmin = 2.1° |
| Absorption correction: multi-scan (REQAB; Rigaku, 1998) | h = −14→14 |
| Tmin = 0.850, Tmax = 1.00 | k = −9→9 |
| 13236 measured reflections | l = −20→20 |
| 2957 independent reflections |
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