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Oxidation of methanol (solvent) with H2O2 catalyzed by 1 (0.25 mM). HCHO was quantified colorimetrically (see the Supporting Information for details). The number of equivalents of H2O2 is with respect to 2. Slow addition of H2O2 indicates a rate of addition of 0.4 equiv min–1 (the two rightmost bars).
