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. 2018 Oct 10;8:15103. doi: 10.1038/s41598-018-32893-2

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© The Author(s) 2018

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(A) Recorded CVs under N₂-saturated (dash line) and O₂-saturated attributed to BOx immobilized on bare Au electrode (a) AuNSs modified Au electrode (b) PTCA-Au electrode prepared by conventional three-electrode system (c) and bipolar electrochemistry method (d) along with schematic of their specific orientations. (B) Recorded CVs under N₂-saturated (dash line) and O₂-saturated for BOx immobilized onto PTCA/Au electrode prepared by BPE in ACN solution with different percent of water 0% (a) 5% (b) 15% (c). (C) CVs attributed to BOx immobilized on PTCA-modified Au electrode under O₂-saturated after 1 cycle (solid line) and after passing some days (dash lines). Experimental condition: 0.1 M PBS, pH = 6, scan rate = 20 mV s⁻¹.