Table 1.
X-ray data collection and refinement statistics.
| Structure | polκ-DNA-dATP* |
|---|---|
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a, b, c (Å) | 67.6, 124.6, 165.0 |
| Resolution (Å)a | 44.1–2.00 (2.11–2.00) |
| Rmerge (%) | 7.0 (55.0) |
| I/σI | 12.0 (2.8) |
| Completeness (%) | 98.3 (97.4) |
| Redundancy | 4.5 (4.7) |
| Refinement | |
| Resolution (Å) | 44.1–2.00 |
| No. reflections | 90,700 |
| Rwork/Rfree (%) | 19.9/23.4 |
| No. atoms | |
| Protein | 6989 |
| DNA | 898 |
| Ligand | 60 |
| Water | 484 |
| B-factors (Å2) | |
| Protein | 42.3 |
| DNA | 41.5 |
| Ligand | 27.1 |
| Water | 42.3 |
| R.m.s. deviations. | |
| Bond lengths (Å) | 0.012 |
| Bond angles (°) | 1.590 |
aValues in parentheses are for the highest resolution shell.