Table 2.
Methodology details for electrochemical-detector-based analysis
| Laboratory | Sample vol. | Sample enrichment |
|---|---|---|
| 3 | 50–100 μl | 1) Bondelut CH column; 2) HPLC system 1; fraction containing 8-oxodG collected |
| 5 | 50 μl | Urine sample diluted 1:1 with 2 × MP1; HPLC system 1: fraction containing 8-oxodG collected (C1, MP1); HPLC system 2; fraction containing 8-oxodG collected (C2, MP2 and MP3) |
| 7 | 500 μl (50 μl injected) | SPE: bond elute C18(OH) (3 ml), bond elute strong cation exchange column (3 ml) |
| 13 | 50 μl (10 μl injected) | SPE: anion exchange column |
Literature references for methodology are provided, where available. MP, mobile phase; C1, column 1; C2, column 2; C3, column 3.