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. 2018 Oct 18;8:15424. doi: 10.1038/s41598-018-32959-1

Table 3.

Verification of stability of Gal antigen-positive reference materials.

Storage conditions of the samples# Gal epitopes (×1014/mg)
# of months stored at −20 °C
  1 6.06 ± 0.20
  6 6.71 ± 0.10
  12 6.97 ± 0.20
# of times of freezing/thawing
  1 6.49 ± 0.62
  3 6.73 ± 0.15
  5 6.48 ± 0.23
# of days stored at 4 °C
  3 6.40 ± 0.49
  7 6.31 ± 0.40
  14 6.16 ± 0.49
  30 5.87 ± 1.02
# of days stored at 25 °C
  3 7.49 ± 0.72
  7 6.70 ± 1.83
  14 7.10 ± 1.19
# of days stored at 37 °C
  1 6.24 ± 1.31
  3 4.34 ± 0.81*
  7 4.67 ± 0.69*

*p < 0.05 compared to the identified value [(6.66 ± 0.83) × 1014/mg] of Gal antigen-positive reference material (stored at −20 °C); #n = 3.