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. Author manuscript; available in PMC: 2019 Dec 24.
Published in final edited form as: Anal Chim Acta. 2018 Aug 28;1041:68–77. doi: 10.1016/j.aca.2018.08.049

Table 3.

Recoveries for CH3Hg+ and Hg2+ for extraction from artificially contaminated soils with dilute HCl and HNO3 via ultrasounds agitation at room temperature. Values are mean ± standard deviation of five replicate extractions (n = 5)

Analyte Medium Sonication time (min)
0 3 6

Recovery (%)
Hg2+ Water 0.95 ± 0.5 8.5 ± 3.2 12 ± 4
5% HCl 24 ± 3 20 ± 5 29 ± 6
10% HCl 58 ± 5 84 ± 6 101 ± 6
5% HNO3 3.5 ± 1.1 4.3 ± 1.8 4.7 ± 3.0
10% HNO3 3.5 ± 1.2 5.5 ± 2.5 8.6 ± 2.0

CH3Hg+ Water 2.1 ± 1.3 33 ± 6 58 ± 5
5% HCl 65 ± 3 86 ± 4 98 ± 2
10% HCl 82 ± 3 102 ± 5 101 ± 3
5% HNO3 71 ± 6 100 ± 4 102 ± 5
10% HNO3 94 ± 5 99 ± 4 104 ± 4