Table 1.
Crystallographic Statistics
| Data collection | |
|---|---|
| X‐ray source | SPring‐8 BL26B1 |
| Detector | R‐AXIS V |
| Wave length (Å) | 0.8 |
| Resolution (Å) | 50.00–1.16 (1.18–1.16) |
| Space group | I4 |
| Unit cell parameters | |
| a, b (Å) | 124.872 |
| c (Å) | 175.683 |
| Total reflections | 1,405,342 |
| Unique reflections | 456,412 (22,818) |
| Completeness (%) | 98.8 (99.0) |
| Redundancy | 3.1 (2.9) |
| Mean I/σ (I) | 26.9 (3.08) |
| R merrge | 0.056 (0.464) |
| R pim | 0.036 (0.327) |
| CC1/2 (highest resolution shell) | 0.729 |
| Refinement | |
| R work/R free | 0.1377/0.1566 |
| No. of atoms/Bfactors (Å2) | |
| Protein | 9351/11.63 |
| Ligands | |
| Ethylene glycol | 200/31.20 |
| Magnesium | 9/37.07 |
| sulfate | 65/67.49 |
| Water | 1007/26.40 |
| RMSD from ideal geometry | |
| Bond lengths (Å) | 0.005 |
| Bond angles (°) | 0.838 |
| Coordinate error (Å) | 0.09 |
| Ramachandran plot | |
| Favored regions (%) | 98.5 |
| Allowed regions (%) | 1.50 |
| Outliners (%) | 0 |
| PDB code | http://firstglance.jmol.org/fg.htm?mol=6A4U |