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. 2018 Oct 17;10(4):72. doi: 10.1007/s40820-018-0223-3

Table 1.

Summary of the advantages and disadvantages of different synthesis methods

Synthesis method Advantages Disadvantages
Laser ablation

Simple experimental setup

Can produce particles with different size by changing experimental parameters

Low yield
Arc discharge Can be obtained from the by-products from purification of carbon nanotubes

Arc-discharged soot contains impurities that are to remove

Expensive equipment

Electrochemical approach

Low cost

High output

Easy manipulation

Doping with heteroatoms is difficult
Chemical oxidation

Requires inexpensive equipment

Large-scale production

Tedious steps

Toxic reagents

Requires strong acid/base

Hydrothermal

Low cost

Easy to manipulate parameters such as temperature, time, and pressure of vessel

Long synthesis duration
Pyrolysis of precursors

Simple procedure

Short synthesis duration

Difficult to achieve high temperatures for aqueous reaction using domestic microwave oven

Simple pyrolysis is difficult to be scaled up due to uneven heating

Broad size distribution

Reverse micelles Can be carry out in room temperature Complicated steps involved
Supported template Uniform particle sizes

Complicated steps involved

Requires additional passivation steps

Difficult to purify