Table 1.
Synthesis method | Advantages | Disadvantages |
---|---|---|
Laser ablation |
Simple experimental setup Can produce particles with different size by changing experimental parameters |
Low yield |
Arc discharge | Can be obtained from the by-products from purification of carbon nanotubes |
Arc-discharged soot contains impurities that are to remove Expensive equipment |
Electrochemical approach |
Low cost High output Easy manipulation |
Doping with heteroatoms is difficult |
Chemical oxidation |
Requires inexpensive equipment Large-scale production |
Tedious steps Toxic reagents Requires strong acid/base |
Hydrothermal |
Low cost Easy to manipulate parameters such as temperature, time, and pressure of vessel |
Long synthesis duration |
Pyrolysis of precursors |
Simple procedure Short synthesis duration |
Difficult to achieve high temperatures for aqueous reaction using domestic microwave oven Simple pyrolysis is difficult to be scaled up due to uneven heating Broad size distribution |
Reverse micelles | Can be carry out in room temperature | Complicated steps involved |
Supported template | Uniform particle sizes |
Complicated steps involved Requires additional passivation steps Difficult to purify |