Table 3. Data collection and processing.
Construct | NPP349–875 |
Beamline | BESSY MX14.1 |
Detector | Rayonix MX225 |
Wavelength (Å) | 0.91841 |
Temperature (K) | 100 |
Rotation range per image (°) | 1 |
Total rotation range (°) | 210 |
Exposure time per image (s) | 7 |
Space group | P1 |
a, b, c (Å) | 76.4, 116.3, 124.2 |
α, β, γ (°) | 86.8, 87.8, 88.2 |
Mosaicity (°) | 0.21 |
Resolution range (Å) | 47.2–2.8 (3.04–2.80) |
Total No. of reflections | 159100 |
No. of unique reflections | 68486 (3424) |
Completeness (%) | 65.2 (14.8) |
Multiplicity | 2.4 (2.6) |
〈I/σ(I)〉 | 9.2 (1.3) |
R p.i.m. (%) | 6.8 (60.3) |
CC1/2 | 0.996 (0.425) |
Overall B factor from Wilson plot (Å2) | 67.4 |
No. of molecules in asymmetric unit | 4 |
Matthews coefficient (Å3 Da−1) | 2.92 |
Solvent content (%) | 57.8 |