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. 2018 Oct 16;74(Pt 11):696–703. doi: 10.1107/S2053230X18011111

Table 3. Data collection and processing.

Construct NPP349–875
Beamline BESSY MX14.1
Detector Rayonix MX225
Wavelength (Å) 0.91841
Temperature (K) 100
Rotation range per image (°) 1
Total rotation range (°) 210
Exposure time per image (s) 7
Space group P1
a, b, c (Å) 76.4, 116.3, 124.2
α, β, γ (°) 86.8, 87.8, 88.2
Mosaicity (°) 0.21
Resolution range (Å) 47.2–2.8 (3.04–2.80)
Total No. of reflections 159100
No. of unique reflections 68486 (3424)
Completeness (%) 65.2 (14.8)
Multiplicity 2.4 (2.6)
I/σ(I)〉 9.2 (1.3)
R p.i.m. (%) 6.8 (60.3)
CC1/2 0.996 (0.425)
Overall B factor from Wilson plot (Å2) 67.4
No. of molecules in asymmetric unit 4
Matthews coefficient (Å3 Da−1) 2.92
Solvent content (%) 57.8