Table 1.
MesoH46L/Q47L | H46L/Q47L | ||||
---|---|---|---|---|---|
Residue | Nucleus | δ (ppm) | T1 (ms) | δ (ppm) | T1 (ms) |
His70 | NH | 10.39 | 10.35 | ||
Hα | 7.97 | 7.80 | |||
Hβ3 | 12.32 | 45 | 12.55 | 35 | |
Hβ2 | 8.02 | 8.10 | |||
N | 120.1 | 119.8 | |||
Cα | 82.9 | 84.8 | |||
Cβ | 22.5 | 22.2 | |||
Hisll7 | NH | 11.49 | 11.23 | ||
Hα | 7.78 | 60 | 7.49 | ||
Hβ3 | 11.70 | 50 | 11.56 | 35 | |
Hβ2 | 8.18 | 8.39 | |||
N | 119.6 | 119.2 | |||
Cα | 73.7 | 74.2 | |||
Cβ | 20.9 | N.D. |
25 °C, 5% 2H2O, pH 7.1. T1 values have a standard error of the fit lower than 5% (Figure S1).