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. 2018 Oct 12;140(43):14455–14463. doi: 10.1021/jacs.8b09326

Table 2. DNP Results Obtained with 8 M [2-13C]DHAc Samples Polarized Using a HyperSense Polarizer with Liquid-State Polarizations Measured 16 s after Dissolution at 7 T.

[2-13C] DHAc doped with build-up time constant (s) liquid-state 13C polarization (%)
(1) PhGA 1033 ± 82 3.1 ± 0.8
(2) PhGA and Gd3+ 1023 ± 97 5.1 ± 1.2
(3) d5-PhGA and Gd3+ 862 ± 81 4.7 ± 1.0
(4) Trityl and Gd3+ 1611 ± 353 16.0 ± 4.0