Table 2. DNP Results Obtained with 8 M [2-13C]DHAc Samples Polarized Using a HyperSense Polarizer with Liquid-State Polarizations Measured 16 s after Dissolution at 7 T.
[2-13C] DHAc doped with | build-up time constant (s) | liquid-state 13C polarization (%) |
---|---|---|
(1) PhGA | 1033 ± 82 | 3.1 ± 0.8 |
(2) PhGA and Gd3+ | 1023 ± 97 | 5.1 ± 1.2 |
(3) d5-PhGA and Gd3+ | 862 ± 81 | 4.7 ± 1.0 |
(4) Trityl and Gd3+ | 1611 ± 353 | 16.0 ± 4.0 |