Skip to main content
. Author manuscript; available in PMC: 2019 Sep 1.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2018 Jul 5;1093-1094:119–127. doi: 10.1016/j.jchromb.2018.07.004

Table 3.

Intra and interassay accuracy and precision of MIH produced by acid hydrolysis of an MIC-protein adduct.

Concentration (mg/kg) Intraassay (within run) Interassay (between run)
Accuracy (%)a Precision (%RSD)a Accuracy (%)b Precision (%RSD)c
Day 1 Day 2 Day 3 Day 1 Day 2 Day 3
0.188 100±1.8 100±3.9 100±2.1 3.6 6.3 8.1 100±2.6 2.3
1.88 100±7.1 100±1.4 100±0.9 5.3 4.9 3.1 100±3.1 2.9
8.75 100±8.0 100±4.1 100±5.1 3.7 2.3 3.9 100±5.7 1.4
a

QC method validation (N = 5).

b

Mean of three different days of QC method validation (N = 15).

c

Between run precision was calculated based on Krouwer and Rabinowitz (43) (N = 15).