Table 1.
X-ray data collection statistics
| Data collection statistics | |
|---|---|
| Temperature (K) | 100 |
| X-ray source | MX2 Australian Synchrotron |
| Spacegroup | P1 |
| Cell dimensions (Å) | 66.9, 122.1, 131.6 |
| 73.1, 82.1, 84.5 | |
| Resolution (Å) | 66.1-2.9 (3.06–2.9) |
| Total number of observations | 233,422 (34,352) |
| No. of unique observations | 80,841 (12,101) |
| Multiplicity | 2.9 (2.8) |
| Data completeness | 92.8 (95.4) |
| I/σI | 6.3 (2.2) |
| 1Rmerge (%) | 0.176 (0.545) |
| Rpim (%) | 0.114 (0.363) |
| Refinement statistics | |
| Non-hydrogen atoms | |
| Protein | 22828 |
| Sugar | 157 |
| Water | 8 |
| 2Rfactor (%) | 20.6 |
| Rfree (%) | 22.5 |
| r.m.s.d from ideality | |
| Bond lengths (Å) | 0.01 |
| Bond angles (°) | 1.13 |
| Ramachandran plot | |
| Favored regions (%) | 93.2 |
| Allowed regions (%) | 6.1 |
| Disallowed regions (%) | 0.7 |
| B factor, all atoms (Å2) | 52.0 |