Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H17NO2 |
| M r | 267.31 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 93 |
| a, b, c (Å) | 5.8354 (5), 16.5123 (14), 15.1330 (12) |
| β (°) | 93.837 (2) |
| V (Å3) | 1454.9 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.25 × 0.18 × 0.14 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS RAPID |
| Absorption correction | Multi-scan (ABSCOR; Higashi, 1995 ▸) |
| T min, T max | 0.642, 0.989 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 13857, 3316, 2572 |
| R int | 0.043 |
| (sin θ/λ)max (Å−1) | 0.648 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.054, 0.143, 1.13 |
| No. of reflections | 3316 |
| No. of parameters | 183 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.36, −0.21 |